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http://hdl.handle.net/2074/958
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| DC Field | Value | Language |
|---|
| contributor.author | Garg, G | - |
| contributor.author | Bobev, S | - |
| contributor.author | Ganguli, A K | - |
| date.accessioned | 2005-10-18T05:52:44Z | - |
| date.available | 2005-10-18T05:52:44Z | - |
| date.issued | 2002 | - |
| identifier.citation | Solid State Ionics, 146(1-2), 195-198 | en |
| identifier.uri | http://eprint.iitd.ac.in/dspace/handle/2074/958 | - |
| description.abstract | Starting from pure metals and sulphur in evacuated silica tubes single crystals of Cu7.38(11)Mn4Sn12S32 and Cu7.07(6)Ni4Sn12S32 have been obtained by quenching from 680 °C. These crystallize in the Fdm space group and have a=10.4145 (7) and 10.305 (1) Å, respectively. The atomic parameters, occupancies and anisotropic thermal parameters were refined to give a final R-value of 0.0209 and 0.0181 for Cu7.38Mn4Sn12S32 and Cu7.07Ni4Sn12S32, respectively. A significant amount of cation deficiency exists at 8a site of the quaternary spinel structure. | en |
| format.extent | 291512 bytes | - |
| format.mimetype | application/pdf | - |
| language.iso | en | en |
| subject | Cation-deficient thiospinel | en |
| subject | Chemical synthesis | en |
| subject | Crystal structure and symmetry | en |
| title | Single crystal structures of two new cation-deficient thiospinels: Cu7.38(11)Mn4Sn12S32 and Cu7.07(6)Ni4Sn12S32 | en |
| type | Article | en |
| Appears in Collections: | Chemistry
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| gargsingl2001.pdf | | 284Kb | Adobe PDF | View/Open |
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