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http://hdl.handle.net/2074/979
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| Title: | Synthesis and NMR study of pyridinocholaphanes |
| Authors: | Pandey, Pramod S
Rai, Roopali
Singh, Rhiddi B |
| Keywords: | steroid
macrocycles
bis-cesium 3,5-pyridine dicarboxylate
DEPT-NMR
HSQC-NMR |
| Issue Date: | 2002 |
| Citation: | Tetrahetron, 58(2), 355-362 |
| Abstract: | Pyridinocholaphanes based on cholic, deoxycholic and lithocholic acids with ethylenediamine and m-xylylenediamine as spacers were synthesized using Cs-salt methodology. Their structures were elucidated on the basis of their IR, NMR and FAB mass spectral data. The NMR techniques, DEPT13C{1H}135/90 and HSQC{1H–13C} were used for the detailed assignment of the carbon atoms of the pyridinocholaphanes. |
| URI: | http://eprint.iitd.ac.in/dspace/handle/2074/979 |
| Appears in Collections: | Chemistry
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| pandaysyn2002.pdf | | 76Kb | Adobe PDF | View/Open |
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