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Please use this identifier to cite or link to this item: http://eprint.iitd.ac.in/handle/2074/979

Title: Synthesis and NMR study of pyridinocholaphanes
Authors: Pandey, Pramod S
Rai, Roopali
Singh, Rhiddi B
Keywords: steroid
macrocycles
bis-cesium 3,5-pyridine dicarboxylate
DEPT-NMR
HSQC-NMR
Issue Date: 2002
Citation: Tetrahetron, 58(2), 355-362
Abstract: Pyridinocholaphanes based on cholic, deoxycholic and lithocholic acids with ethylenediamine and m-xylylenediamine as spacers were synthesized using Cs-salt methodology. Their structures were elucidated on the basis of their IR, NMR and FAB mass spectral data. The NMR techniques, DEPT13C{1H}135/90 and HSQC{1H–13C} were used for the detailed assignment of the carbon atoms of the pyridinocholaphanes.
URI: http://eprint.iitd.ac.in/dspace/handle/2074/979
Appears in Collections:Chemistry

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