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Single crystal structure and Mössbauer studies of a new cation-deficient thiospinel: Cu5.47Fe2.9Sn13.1S32
Starting from pure metals and sulphur in evacuated silica tubes single crystals of Cu5.47(9)Fe2.9(3)Sn13.1(3)S32 have been obtained by quenching from 680°C. It crystallizes in the Fdm space group with a = 10.3022 (6) Å. ...